Effect of Anodizing Process Conditions on Electrical Characteristics of Sintered Tantalum Nitride Anodes
Received:February 21, 2012   Revised:February 21, 2012   Accepted:February 23, 2012      Published Online:August 20, 2012
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DOI:doi:10.3969/j.issn.1007-7545.2012.09.014
KeyWord:sintered tantalum nitride anodes; electrical characteristics; anodization
           
AuthorInstitution
Liu Lianyun 北京科技大学冶金与生态工程学院;北京交通大学理学院
Duan Shiyu 山东省冶金设计院股份有限公司
Huang Kai 北京科技大学冶金与生态工程学院
Zhu Hongmin 北京科技大学冶金与生态工程学院
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Abstract:
      Sintered tantalum nitride anodes were prepared with tantalum nitride nanopowders. The sintered anode slugs were examined by XRD. The effects of formation solution in terms of its variety, concentration and temperature, current density and formation voltage on electrical characteristics were studied. The results show that the anode slugs are made of pure tantalum nitride phase, and the optimum anodizing process conditions including H3PO4 concentration of 0.01%, temperature of formation solutions of 55 ℃, current density of 40 mA/g and the formation voltage of less than 16 V.
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