Preparation and Characterizations of Ba0.2Ca0.8TiO3:Pr Nano-Powder
Received:November 30, 2012   Revised:December 06, 2012   Accepted:December 06, 2012      Published Online:June 19, 2013
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DOI:10.3969/j.issn.1007-7545.2013.07.014
KeyWord:Ca0.8 Ba0.2TiO3:Pr; sol-gel; luminescent materials; nano-powder; preparation
                 
AuthorInstitution
mou yan nan 黑河学院
Qiu Min 黑河学院
Pi Yan Mei 黑河学院
Zhang Xiu Ping 黑河学院
Yang Yu Rong 黑河学院
Liu Ping 黑河学院
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Abstract:
      Ba0.2Ca0.8TiO3:Pr nano-powders were prepared with sol-gel method and their structure, morphology and photoluminescence properties were characterized by XRD, SEM and fluorescence spectrophotometer, respectively. The results show that the as-prepared Ca0.8Ba0.2Ti03:Pr3 powders are spherical with submicron particle size. The particles sintered at 900 ℃ for eight hours show a strong red emission (main peak 612 nm), which can be assigned to be a typical 1D2→3H4 transition of Pr3 . The sample treated at a higher temperature (900 ℃) presents the highest initial luminescent intensity and longest decay time.
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