Study on Palladium Separation by Solid Phase Extraction with Bicine
Received:May 03, 2013   Revised:May 04, 2013   Accepted:May 06, 2013      Published Online:October 25, 2013
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DOI:10.3969/j.issn.1007-7545.2013.11.010
KeyWord:MCI-GEL resin; solid-phase extraction; palladium; enrichment; Bicine
        
AuthorInstitution
linhuikun 德宏师范高等专科学校理工系
yangxinzhou 德宏师范高等专科学校理工系;
yangzixian 德宏师范高等专科学校理工系
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Abstract:
      The behavior of and conditions for separation and enrichment of palladium from metal-ions by MCI-GEL resin were studied. The results show that the complex compound formed by palladium and Bicine can be adsorbed by MCI-GEL resin. Palladium could be quantitatively separated from Pt(Ⅳ), Fe(Ⅲ), Ni(Ⅱ), Cu(Ⅱ), Zn(Ⅱ) by extraction with palladium extraction rate of above 99% under the conditions including molar ratio of Bicine and palladium of 2∶1, hydrochloric acid concentrations of 0.01 mol/L and column flow rate of 10 mL/min.
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