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| Synthesis of Tetrammine Palladium (II) Sulphate by Ion Exchange Method |
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Received:September 15, 2015
Revised:September 17, 2015
Accepted:September 18, 2015
Published Online:February 23, 2016
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| DOI：10.3969/j.issn.1007-7545.2016.03.015 |
| KeyWord:tetrammine palladium(II) sulphate; ion exchange; synthesis; recovery |
| Author | Institution |
| WANG Huan |
贵研资源易门有限公司 |
| HE Xiaotang |
贵研资源易门有限公司 |
| WU Xilong |
贵研资源易门有限公司 |
| HAN Shouli |
贵研资源易门有限公司 |
| ZHAO Yu |
贵研资源易门有限公司 |
| LI Zixuan |
贵研资源易门有限公司 |
| LIAO Wei |
昆明贵金属研究所 |
| LEI Ting |
昆明冶金高等专科学校 |
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| Abstract: |
| Tetrammine palladium(II) sulphate was synthesized from palladium chloride by complexation with ammonium hydroxide, ion exchange, neutralization with sulfuric acid, and recrystallization purification. Its characteristic components were analyzed. The results show that high purity tetrammine palladium(II) sulphate was obtained by ion exchange process with overall yield rate of 86.82%, suitable for commercial production. |
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