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| New Technology for Preparation of High Compacted Density Palladium Powder by Chemical Reduction Method |
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Received:April 15, 2024
Revised:April 27, 2024
Accepted:May 06, 2024
Published Online:July 09, 2024
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| DOI:doi:10.3969/j.issn.1007-7545.2024.08.010 |
| KeyWord:chemical reduction method; hydrazine dihydrochloride; refine; high compacted density palladium powder |
| Author | Institution |
| CHEN Zhiyu |
金川集团上海金属资源有限公司 |
| WANG Deyu |
金川集团铜贵有限公司 |
| PAN Congming |
金川集团铜贵有限公司 |
| GAO Xiangqian |
金川集团铜贵有限公司 |
| FANG Xiao |
金川集团铜贵有限公司 |
| LI Li |
金川集团铜贵有限公司 |
| LI Rui |
金川集团铜贵有限公司 |
| BAI Weidao |
金川集团铜贵有限公司 |
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| Abstract: |
| The particle size and density of high compacted density palladium powder prepared under different conditions were investigated by using the complex solution in the refining process of platinum group metal palladium as raw material, and the optimal preparation process and technical conditions were selected through experiments.
The results show that high compacted density palladium powders with uniform particles and compacted density up to about 3.25 g/cm3 can be prepared by direct reduction of palladium complex solution with hydrazine hydrate to form palladium sponge as crystal seed at pH=8 and further reduction with hydrazine dihydrochloride. |
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